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Extra resources for Argumentation, Study of Effective Reasoning. Guild 2
Sample text
Tests on an accelerating rate calorimeter (ARC) showed the onset of decomposition at 130 C, with DHdec ¼ 278 J gÀ1 , and a final temperature of 179 C. 2 Phosgene ‘‘Oligomers’’ below the boiling point, although there is no evidence of its decomposition below 130 C [16]. To identify the gases produced from the decomposition of triphosgene, an experiment was performed on a thermogravimetric analyzer interfaced to a Fourier transform infrared spectrometer (TGA-FTIR) [16]. The simultaneous presence of phosgene, diphosgene, carbon dioxide, and tetrachloromethane among the thermal decomposition products suggested another decomposition mechanism, which would be favored by a six-membered transition state, as shown below.
01 mol) was condensed at À50 C. 5 h. The reaction mixture was stirred for a further 12 h at 0 C (ice bath), with monitoring of the reaction by TLC. Thereafter, the cooling bath was replaced by an oil bath and the flask was fitted with a distillation apparatus. 03 Torr). Analyses (1 H and 13 C NMR, IR, TLC) were indicative of a pure product (free from benzyl chloride). Important: During the course of the distillation, the temperature of the oil bath must be kept below 65 C! At higher temperatures, benzyl chloride will be increasingly generated.
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